Automated electron diffraction tomography - Development and applications

Ute Kolb; Yaşar Krysiak; Sergi Plana-Ruiz

doi:10.1107/S2052520619006711

Automated electron diffraction tomography - Development and applications

Ute Kolb^*, Yaşar Krysiak, Sergi Plana-Ruiz

^*Corresponding author for this work

Research output: Contribution to journal › Article › Research › peer review

Abstract

Electron diffraction tomography (EDT) has gained increasing interest, starting with the development of automated electron diffraction tomography (ADT) which enables the collection of three-dimensional electron diffraction data from nano-sized crystals suitable for ab initio structure analysis. A basic description of the ADT method, nowadays recognized as a reliable and established method, as well as its special features and general applicability to different transmission electron microscopes is provided. In addition, the usability of ADT for crystal structure analysis of single nano-sized crystals with and without special crystallographic features, such as twinning, modulations and disorder is demonstrated.

Original language	English
Pages (from-to)	463-474
Number of pages	12
Journal	Acta Crystallographica Section B: Structural Science, Crystal Engineering and Materials
Volume	75
DOIs	https://doi.org/10.1107/S2052520619006711
Publication status	Published - 1 Aug 2019
Externally published	Yes

Keywords

disorder analysis
electron crystallography
electron diffraction tomography
nanomaterials
single-crystal structure analysis

ASJC Scopus subject areas

Electronic, Optical and Magnetic Materials
Atomic and Molecular Physics, and Optics
Metals and Alloys
Materials Chemistry

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10.1107/S2052520619006711

Cite this

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title = "Automated electron diffraction tomography - Development and applications",

abstract = "Electron diffraction tomography (EDT) has gained increasing interest, starting with the development of automated electron diffraction tomography (ADT) which enables the collection of three-dimensional electron diffraction data from nano-sized crystals suitable for ab initio structure analysis. A basic description of the ADT method, nowadays recognized as a reliable and established method, as well as its special features and general applicability to different transmission electron microscopes is provided. In addition, the usability of ADT for crystal structure analysis of single nano-sized crystals with and without special crystallographic features, such as twinning, modulations and disorder is demonstrated.",

keywords = "disorder analysis, electron crystallography, electron diffraction tomography, nanomaterials, single-crystal structure analysis",

author = "Ute Kolb and Ya{\c s}ar Krysiak and Sergi Plana-Ruiz",

note = "Funding information: The following funding is acknowledged: Stipendienstiftung of federal state of Rhineland-Palatinate (grant to Yasar Krysiak); Johannes Gutenberg-Universit{\"a}t Mainz (grant to Yasar Krysiak).",

year = "2019",

month = aug,

day = "1",

doi = "10.1107/S2052520619006711",

language = "English",

volume = "75",

pages = "463--474",

journal = "Acta Crystallographica Section B: Structural Science, Crystal Engineering and Materials",

issn = "2052-5192",

publisher = "John Wiley & Sons Inc.",

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TY - JOUR

T1 - Automated electron diffraction tomography - Development and applications

AU - Kolb, Ute

AU - Krysiak, Yaşar

AU - Plana-Ruiz, Sergi

N1 - Funding information: The following funding is acknowledged: Stipendienstiftung of federal state of Rhineland-Palatinate (grant to Yasar Krysiak); Johannes Gutenberg-Universität Mainz (grant to Yasar Krysiak).

PY - 2019/8/1

Y1 - 2019/8/1

N2 - Electron diffraction tomography (EDT) has gained increasing interest, starting with the development of automated electron diffraction tomography (ADT) which enables the collection of three-dimensional electron diffraction data from nano-sized crystals suitable for ab initio structure analysis. A basic description of the ADT method, nowadays recognized as a reliable and established method, as well as its special features and general applicability to different transmission electron microscopes is provided. In addition, the usability of ADT for crystal structure analysis of single nano-sized crystals with and without special crystallographic features, such as twinning, modulations and disorder is demonstrated.

AB - Electron diffraction tomography (EDT) has gained increasing interest, starting with the development of automated electron diffraction tomography (ADT) which enables the collection of three-dimensional electron diffraction data from nano-sized crystals suitable for ab initio structure analysis. A basic description of the ADT method, nowadays recognized as a reliable and established method, as well as its special features and general applicability to different transmission electron microscopes is provided. In addition, the usability of ADT for crystal structure analysis of single nano-sized crystals with and without special crystallographic features, such as twinning, modulations and disorder is demonstrated.

KW - disorder analysis

KW - electron crystallography

KW - electron diffraction tomography

KW - nanomaterials

KW - single-crystal structure analysis

UR - http://www.scopus.com/inward/record.url?scp=85070601984&partnerID=8YFLogxK

U2 - 10.1107/S2052520619006711

DO - 10.1107/S2052520619006711

M3 - Article

C2 - 32830704

AN - SCOPUS:85070601984

SN - 2052-5192

VL - 75

SP - 463

EP - 474

JO - Acta Crystallographica Section B: Structural Science, Crystal Engineering and Materials

JF - Acta Crystallographica Section B: Structural Science, Crystal Engineering and Materials

ER -

Automated electron diffraction tomography - Development and applications

Abstract

Keywords

ASJC Scopus subject areas

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