M-iodosylbenzoic acid: Recyclable hypervalent iodine reagent for-tosyloxylation and-mesyloxylation of ketones

Mekhman S. Yusubov; Tatyana V. Funk; Roza Y. Yusubova; Galina Zholobova; Andreas Kirschning; Joo Yeon Park; Ki Whan Chi

doi:10.1080/00397910902838870

M-iodosylbenzoic acid: Recyclable hypervalent iodine reagent for-tosyloxylation and-mesyloxylation of ketones

Mekhman S. Yusubov
, Tatyana V. Funk
, Roza Y. Yusubova
, Galina Zholobova
, Andreas Kirschning
, Joo Yeon Park
, Ki Whan Chi

Research output: Contribution to journal › Article › Research › peer review

Abstract

m-Iodosylbenzoic acid-mediated reactions of various carbonyl compounds provided-organosulfonyloxy carbonyl compounds in good yields. The final products could be easily isolated without any chromatographic purification by simple treatment of the crude mixture with an anionic exchange resin.

Original language	English
Pages (from-to)	3772-3784
Number of pages	13
Journal	Synthetic Communications
Volume	39
Issue number	21
DOIs	https://doi.org/10.1080/00397910902838870
Publication status	Published - Jan 2009

Keywords

-organosulfonyloxy ketones
-sulfonylation of ketones
Hypervalent iodine
Recycle

ASJC Scopus subject areas

Organic Chemistry

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10.1080/00397910902838870

Cite this

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title = "M-iodosylbenzoic acid: Recyclable hypervalent iodine reagent for-tosyloxylation and-mesyloxylation of ketones",

abstract = "m-Iodosylbenzoic acid-mediated reactions of various carbonyl compounds provided-organosulfonyloxy carbonyl compounds in good yields. The final products could be easily isolated without any chromatographic purification by simple treatment of the crude mixture with an anionic exchange resin.",

keywords = "-organosulfonyloxy ketones, -sulfonylation of ketones, Hypervalent iodine, Recycle",

author = "Yusubov, \{Mekhman S.\} and Funk, \{Tatyana V.\} and Yusubova, \{Roza Y.\} and Galina Zholobova and Andreas Kirschning and Park, \{Joo Yeon\} and Chi, \{Ki Whan\}",

note = "Funding information: M. S. Y. and A. K. thank Fonds der Chemischen Industrie for support of this work. K. W. C., M. S. Y., and R. Y. Y. are grateful for the support of the Brain Korea 21 program.",

year = "2009",

month = jan,

doi = "10.1080/00397910902838870",

language = "English",

volume = "39",

pages = "3772--3784",

journal = "Synthetic Communications",

issn = "0039-7911",

publisher = "Taylor and Francis Ltd.",

number = "21",

}

TY - JOUR

T1 - M-iodosylbenzoic acid

T2 - Recyclable hypervalent iodine reagent for-tosyloxylation and-mesyloxylation of ketones

AU - Yusubov, Mekhman S.

AU - Funk, Tatyana V.

AU - Yusubova, Roza Y.

AU - Zholobova, Galina

AU - Kirschning, Andreas

AU - Park, Joo Yeon

AU - Chi, Ki Whan

N1 - Funding information: M. S. Y. and A. K. thank Fonds der Chemischen Industrie for support of this work. K. W. C., M. S. Y., and R. Y. Y. are grateful for the support of the Brain Korea 21 program.

PY - 2009/1

Y1 - 2009/1

N2 - m-Iodosylbenzoic acid-mediated reactions of various carbonyl compounds provided-organosulfonyloxy carbonyl compounds in good yields. The final products could be easily isolated without any chromatographic purification by simple treatment of the crude mixture with an anionic exchange resin.

AB - m-Iodosylbenzoic acid-mediated reactions of various carbonyl compounds provided-organosulfonyloxy carbonyl compounds in good yields. The final products could be easily isolated without any chromatographic purification by simple treatment of the crude mixture with an anionic exchange resin.

KW - -organosulfonyloxy ketones

KW - -sulfonylation of ketones

KW - Hypervalent iodine

KW - Recycle

UR - https://www.scopus.com/pages/publications/70349934722

U2 - 10.1080/00397910902838870

DO - 10.1080/00397910902838870

M3 - Article

AN - SCOPUS:70349934722

SN - 0039-7911

VL - 39

SP - 3772

EP - 3784

JO - Synthetic Communications

JF - Synthetic Communications

IS - 21

ER -

M-iodosylbenzoic acid: Recyclable hypervalent iodine reagent for-tosyloxylation and-mesyloxylation of ketones

Abstract

Keywords

ASJC Scopus subject areas

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